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Chemistry Forums for Students => Organic Chemistry Forum => Topic started by: Steem_Russia on August 19, 2006, 02:22:09 PM

Title: NMR P-31
Post by: Steem_Russia on August 19, 2006, 02:22:09 PM
Hello.
I'm lookind for any handboot of NMR-P31 shifts.
What can you recommend to me?
Title: Re: NMR P-31
Post by: sjb on August 20, 2006, 07:29:45 AM
Hello.
I'm lookind for any handboot of NMR-P31 shifts.
What can you recommend to me?

What actually are you after? Perhaps http://fluorine.ch.umist.ac.uk/research/p31calc.php might be useful for phosphines, or something like http://www.amazon.co.uk/gp/product/3540678158/202-5909964-8108647?v=glance&n=266239&v=glance - Pretsch et. al. ?
Title: Re: NMR P-31
Post by: Steem_Russia on August 20, 2006, 02:16:48 PM
I need to have large database of shifts that included phosphines, phosphineoxydes, phosthinates. We are obtaining variety of compaunds and we ned to clean and to see it from NMR-P31, or indentify all compaunds in solution.
Title: Re: NMR P-31
Post by: movies on August 20, 2006, 07:53:24 PM
The Pretsch book has very little on 31P NMR.  In fact, none of my typical NMR reference books have a good list of typical phosphorus shifts, unfortunately.
Title: Re: NMR P-31
Post by: sjb on August 21, 2006, 03:53:50 AM
The Pretsch book has very little on 31P NMR.  In fact, none of my typical NMR reference books have a good list of typical phosphorus shifts, unfortunately.

Doesn't it? Must be thinking of, of misremembering something else then - my copy is ~ 100 miles away at the moment... Thanks

S
Title: Re: NMR P-31
Post by: TheBigF on October 08, 2007, 07:14:41 PM
The UMIST web address given here:
http://fluorine.ch.umist.ac.uk/research/p31calc.php
is out of date. It should now be a Manchester (man) address, viz:
http://fluorine.ch.man.ac.uk/research/p31calc.php

The BigF
Title: Re: NMR P-31
Post by: sjb on October 13, 2007, 05:13:38 AM
The UMIST web address given here:
http://fluorine.ch.umist.ac.uk/research/p31calc.php
is out of date. It should now be a Manchester (man) address, viz:
http://fluorine.ch.man.ac.uk/research/p31calc.php

The BigF

Good catch! I was rather hoping that either the pages would be silently redirected, or at least a page to say UMIST is now part of the University of Manchester.

S