December 30, 2024, 11:10:18 AM
Forum Rules: Read This Before Posting


« previous next »
Pages: [1]   Go Down

Topic: How to remove TBAF  (Read 7838 times)

0 Members and 1 Guest are viewing this topic.

Offline nottingham

  • Regular Member
  • ***
  • Posts: 11
  • Mole Snacks: +0/-0
How to remove TBAF
« on: August 16, 2006, 03:06:30 PM »
difficult to remove the TBAF by washing with water during the workup or flash chromatography.Any ideas?
« Last Edit: September 30, 2006, 04:11:46 AM by Mitch »
Logged

Offline connor

  • Very New Member
  • *
  • Posts: 2
  • Mole Snacks: +0/-0
Re: How to remove TBAF
« Reply #1 on: September 30, 2006, 12:05:09 AM »
Try to crash it out with diethyl ether (provided your product is soluble). I had similar problems when  I worked with tetrabutylmmonium tetrafluoroborate, and this method was easy and efficient.

Logged
Pages: [1]   Go Up
« previous next »
Sponsored Links