December 21, 2024, 08:04:10 PM
Forum Rules: Read This Before Posting


Topic: recrystallization of complex Fe  (Read 3031 times)

0 Members and 1 Guest are viewing this topic.

Offline Diplomania

  • Very New Member
  • *
  • Posts: 1
  • Mole Snacks: +0/-0
recrystallization of complex Fe
« on: February 22, 2016, 06:37:45 AM »
I need a solvent for recrystallization for 1)potassium ferric oxalate trihydrate and for 2) Sodium iron EDTA.
I was thinking of using water for potassium ferric oxalate trihydrate, but I have trouble figuring out what to use for the iron EDTA since it is soluble in water at room temp. I cant. use water. Are there a method to use for choocing the right solvent ?

thankyou

Offline Arkcon

  • Retired Staff
  • Sr. Member
  • *
  • Posts: 7367
  • Mole Snacks: +533/-147
Re: recrystallization of complex Fe
« Reply #1 on: February 23, 2016, 08:48:40 AM »
The crystallization process for KFe-oxalate is given here: https://en.wikipedia.org/wiki/Potassium_ferrioxalate#Preparation

It seems it is crystallized simply by evaporation of the water.  Since Na-Fe-EDTA is likewise sold as a powder, by Sigma-Aldrich, it may very well be made the same way.  I wasn't sure to begin with that it was possible, some complexes may only exist in water solution.  Why do you feel the need to recrystalize?
Hey, I'm not judging.  I just like to shoot straight.  I'm a man of science.

Sponsored Links