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Topic: need your help-synthesiof Grinard reaction  (Read 2363 times)

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Offline bhkuk

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need your help-synthesiof Grinard reaction
« on: March 22, 2008, 12:48:35 AM »
i am making areaction with (-)Menthyl (R)-p-toluenesulfinate with methylmagnesium iodide, the reaction thake place at anhydrous benzene. after doing the reaction i am making hydrolyse with ammonium chloride.
 
after hydrolize of the product ,i should then evaporate my solvent (ether)
after evaporation i add hot hexane till watching white cloudy
i should cold it for the night at -5C and then filtrate it.
the crystals i get i should dissolve at minimum of hot ether and then adding hot n-hexane untill i will see again white cloud, i should cool it again to -5C and the n filtrate and pack the crystals
what happened in this process? why should i do this procedure?

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