December 28, 2024, 05:31:37 AM
Forum Rules: Read This Before Posting


Topic: p-chloro-m-xylenol--has anyone ever tried to analyze a liquid sample for it?  (Read 3889 times)

0 Members and 1 Guest are viewing this topic.

Offline Golden_4_Life

  • Full Member
  • ****
  • Posts: 131
  • Mole Snacks: +3/-4
  • Gender: Female
We are planning to use p-chloro-m-xylenol or "pcmx" as a biocide in one of our bathing solutions; however, we are not sure on how to analyze for it.
Given that it's boiling point is 246 deg C--it would seem unfeasible to test it using a gas chromatograph.  Or would it be feasible?  Has anyone ever attempted to quantify ''pcmx'' via GC?  Or would a more suitable method be via HPLC since this cmpd is not easily volatized?
I have conducted a literature search on the cmpd but info is scant at best.
Any of you analytical chemists ever tried such?

Sincerely,
Golden
Golden4Life

Offline Don Shelly

  • Regular Member
  • ***
  • Posts: 29
  • Mole Snacks: +2/-1
  • I am a professional in the SPE business.
    • UCT website
I recommend either heated purge and trap GC, headspace GC, or SPME GC.

Don

Offline Golden_4_Life

  • Full Member
  • ****
  • Posts: 131
  • Mole Snacks: +3/-4
  • Gender: Female
thanky D.Shelley: I don't know what a purge n trap or spe GC are? I have only access in our lab to a agilent 6890 gc fitted with a capillary column; however, I shall aim to learn what the purge n trap, headspace are as types.
Golden4Life

Sponsored Links