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Topic: how do I purify a thiosemicarbazone ligand?  (Read 3550 times)

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Offline smurf88

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how do I purify a thiosemicarbazone ligand?
« on: January 20, 2010, 02:07:47 AM »
I am trying to produce a semicarbazone ligand.
The melting point should be around 145 to 146 Celcius.
But the ligand that I obtained is around 196C.
I tried to purify it by washing with methanol.
Or is there any better method to purify my ligand?
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Offline verpa

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Re: how do I purify a thiosemicarbazone ligand?
« Reply #1 on: April 02, 2010, 11:32:19 AM »
This one is a bit old ( was just checking out your other posts ) but if you have this sort of question in the future, you might also cross post to:
http://lab.chempedia.com

fwiw.
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