November 28, 2024, 05:24:17 PM
Forum Rules: Read This Before Posting


Topic: Encasing liquified chlorine in an ampoule then in resin  (Read 5063 times)

0 Members and 1 Guest are viewing this topic.

Offline nj_bartel

  • Sr. Member
  • *****
  • Posts: 1487
  • Mole Snacks: +76/-42
Encasing liquified chlorine in an ampoule then in resin
« on: June 10, 2010, 12:20:59 AM »
This was a project I was undertaking, but after a few "dry runs" of practicing the ampoule sealing with water instead of chlorine, I'm realizing that this is beyond my skill level and there's a fairly good chance I'd end up shooting myself in the face with a pretty high concentration of gaseous chlorine.

I've looked online, but have only been able to find a private copy of what I was planning.  Do any of you know someone who might sell/make these?

Offline skyjumper

  • 1,3,7-trimethylxanthine
  • Full Member
  • ****
  • Posts: 167
  • Mole Snacks: +3/-4
  • Gender: Male
  • Lab Aid
Re: Encasing liquified chlorine in an ampoule then in resin
« Reply #1 on: June 10, 2010, 10:40:07 PM »
Try making your ampule out of a longer test tube, more space between where you are working and the actual product. I would be concerned about the pressure needed to liquefy at room temp. probably breaking glass... 

Offline nj_bartel

  • Sr. Member
  • *****
  • Posts: 1487
  • Mole Snacks: +76/-42
Re: Encasing liquified chlorine in an ampoule then in resin
« Reply #2 on: June 11, 2010, 02:26:19 AM »
Chlorine is "easily" condensed with dry ice.  I'll try giving that a shot.  It's hard to work with the flame too near the fingertips though!

Offline vmelkon

  • Chemist
  • Full Member
  • *
  • Posts: 474
  • Mole Snacks: +28/-10
  • Gender: Male
Re: Encasing liquified chlorine in an ampoule then in resin
« Reply #3 on: July 19, 2010, 10:26:04 PM »
I hope your ampule has a small diameter with relatively thick walls.

Offline nj_bartel

  • Sr. Member
  • *****
  • Posts: 1487
  • Mole Snacks: +76/-42
Re: Encasing liquified chlorine in an ampoule then in resin
« Reply #4 on: July 20, 2010, 03:56:13 PM »
Found someone who sold me a quartz ampoule with burst pressure ca 100 atm; encased it myself

Sponsored Links