November 21, 2024, 12:59:14 PM
Forum Rules: Read This Before Posting


« previous next »
Pages: [1]   Go Down

Topic: Imine base synthesis question  (Read 4654 times)

0 Members and 1 Guest are viewing this topic.

Offline SBJ

  • Very New Member
  • *
  • Posts: 2
  • Mole Snacks: +0/-0
Imine base synthesis question
« on: November 27, 2010, 03:28:45 AM »
I am trying to synthesize imine bases of a heterocyclic compound containing both N and S in its cyclic structure, and an amino group is attached to the C between the S and N using various benzaldehydes. Even after refluxing for 5-6 hours i am getting solid product which immediately gets liquified on filteration. Whereas when i reflux for 2-3 hours i am not getting any solid product at all. Can you please suggest any modifications or the reason of why i am not getting the product?
Logged

Offline MissPhosgene

  • Chemist
  • Full Member
  • *
  • Posts: 364
  • Mole Snacks: +23/-5
  • Gender: Female
Re: Imine base synthesis question
« Reply #1 on: November 27, 2010, 10:41:54 AM »
What exactly do you start with and what are the reaction conditions (solvent etc)?
Logged
Stereograms of the 32 crystallographic point groups: little bike wheels of cold, hard, pure rationality.
Pages: [1]   Go Up
« previous next »
Sponsored Links