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Topic: Synthesis Of CuCL2 (DMSO)2  (Read 13122 times)

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Offline fenor

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Synthesis Of CuCL2 (DMSO)2
« on: January 28, 2012, 11:08:20 PM »
Hi,

I have taken 1.9812g of CuCl2 and have added 3 mol equivalent of DMSO (1.104g cm-3).
Now I have to find the theoretical yield. I have done the calculation for it but it does not seem right to me.

Steps:

CuCl2 + 2DMSO → CuCl2*2DMSO

1.9812gCuCl2 / 134.45g * 290.5g CuCl2·2DMSO( molecular weight) which comes to 4.280g

am I doing this right for the theoretical yield?
I have to get the percent yield.

thank you

Offline Borek

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Re: Synthesis Of CuCL2 (DMSO)2
« Reply #1 on: January 29, 2012, 05:04:59 AM »
Assuming you added excess DMSO (and CuCl2 was a limiting reagent, your wording is not clear to me) that's OK.
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Offline fenor

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Re: Synthesis Of CuCL2 (DMSO)2
« Reply #2 on: January 29, 2012, 11:23:42 AM »
I have to calculate the percent yield, the theoretical yield that i got does not seem right to me : 4.280g, since my actual yield is 4.787g. Is this more clear?

In the lab 1.9812 g of CUCl2 mixed with ethanol to be completly mixed then 3 mol equivalent of DMSO was added. The density of DMSO is (1.104g cm-3). Then precipitate was formed and then filtered. The final product that was obtained was 4.787g.


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