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Topic: 2D NMR  (Read 4202 times)

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Offline che-mistry

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2D NMR
« on: November 12, 2012, 04:43:27 PM »
Hello,

How to solve NOESY spectrum and How to assign the coupling constants (for example dddd).

looking forward to more info ....Thanks

Offline Dan

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Re: 2D NMR
« Reply #1 on: November 12, 2012, 04:57:22 PM »
Your question is too broad for an internet forum. Get a book about organic spectroscopy from your library, some general organic texts even have a chapter on this - it is too much material to be reproduced here. Have a read and then come back with more specific questions.

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Examples of books:

http://www.amazon.co.uk/Organic-Spectroscopy-William-Kemp/dp/033351954X
http://www.amazon.co.uk/Introduction-Organic-Spectroscopy-Chemistry-Primers/dp/0198557558
http://www.amazon.co.uk/Understanding-NMR-Spectroscopy-James-Keeler/dp/0470017872

You can probably also find decent NMR tutorials on the web with a bit of googling. Possibly useful search terms might be "NMR splitting patterns", "2D NMR correlation experiments", "nuclear Overhauser effect" etc., but I would recommend getting a textbook that will start you off with the basics (like splitting patterns) and logically guide you to more complicated areas (like 2D NMR and NOE).
My research: Google Scholar and Researchgate

Offline che-mistry

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Re: 2D NMR
« Reply #2 on: November 13, 2012, 03:55:26 AM »
Thank you very much



Your question is too broad for an internet forum. Get a book about organic spectroscopy from your library, some general organic texts even have a chapter on this - it is too much material to be reproduced here. Have a read and then come back with more specific questions.

NB: Forum Rules

Examples of books:

http://www.amazon.co.uk/Organic-Spectroscopy-William-Kemp/dp/033351954X
http://www.amazon.co.uk/Introduction-Organic-Spectroscopy-Chemistry-Primers/dp/0198557558
http://www.amazon.co.uk/Understanding-NMR-Spectroscopy-James-Keeler/dp/0470017872

You can probably also find decent NMR tutorials on the web with a bit of googling. Possibly useful search terms might be "NMR splitting patterns", "2D NMR correlation experiments", "nuclear Overhauser effect" etc., but I would recommend getting a textbook that will start you off with the basics (like splitting patterns) and logically guide you to more complicated areas (like 2D NMR and NOE).

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