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making HCL-DIOXANE please help
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Topic: making HCL-DIOXANE please help (Read 10994 times)
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Snake
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making HCL-DIOXANE please help
«
on:
May 31, 2006, 12:19:31 PM »
Anyone out there knows how to make 4M HCL-dioxane from 37% HCL and 1,4-dioxane?
Please help.
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Snake
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Re: making HCL-DIOXANE please help
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Reply #1 on:
June 01, 2006, 03:30:51 AM »
No one replied...found a way to generate the hcl-dioxane, by adding acetyl chloride with methanol to genrate hcl and then add dioxane to it... dono whether it works trying it now =)
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AWK
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Re: making HCL-DIOXANE please help
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Reply #2 on:
June 01, 2006, 05:27:36 AM »
You ought to use dry gaseous HCl, you can obtain it from solid NaCl + conc. H2SO4
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AWK
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making HCL-DIOXANE please help