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Topic: Orange gas from Nickel dissolution  (Read 2371 times)

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Offline Muonium

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Orange gas from Nickel dissolution
« on: August 17, 2018, 10:19:24 PM »
Hi everyone! After putting Nickel metal in a concentrated hydrochloric acid and 3% hydrogen peroxide solution and heating it, I noticed brownish orange-yellow fumes filling the flask. There was gas production even after the liquid as cooled down.

Could Nickel in NiCl2 catalyses a decomposition reaction of the HCl and produce chlorine or byproducts like chlorine oxides?

The gas smell like HCl and a bit like sodium hypochlorite.

Thanks a lot!

Offline chenbeier

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Re: Orange gas from Nickel dissolution
« Reply #1 on: August 18, 2018, 05:51:10 AM »
The problem was the peroxide. HCl and H2O2 creates chlorine gas.

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