the fischer indole synthesis which i am doing has phenylhydrazine and 4-piperidone as starting materials and the acid catalyst used was gas dry hcl gas.
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the final product is amine salt at the same time it contains 1 equivalent of nh4cl as by product
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i dont want to change the catalyst. can anyone tell me how to prevent the nh4cl formation during the reaction or getting the free amine as final product with out nh4cl
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recrystallization methods to NH4Cl will also be good
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