January 10, 2025, 08:33:56 AM
Forum Rules: Read This Before Posting


Topic: Purpose of adding sodium sulfite to a solution before extraction  (Read 6395 times)

0 Members and 1 Guest are viewing this topic.

Offline tcraw033

  • Regular Member
  • ***
  • Posts: 17
  • Mole Snacks: +0/-0
Hi
So my question is what is the role of the solutions of Na2SO3, Na2CO3, and NaCl in the isolation of the product.  (the lab is on expoxidation of (R)-(--)-Carvone with MCPBA)
So far I know that NaCl and Na2CO3 are used for drying agents and they are what we wash the organic layer with but we add 10% sodium sulfite to the solution before we do an extraction.  I was doing some research and I think it could be to make the reaction irreversible....But im not sure. I would love some advice.
THanks!

Offline sjb

  • Global Moderator
  • Sr. Member
  • ***
  • Posts: 3653
  • Mole Snacks: +222/-42
  • Gender: Male
Re: Purpose of adding sodium sulfite to a solution before extraction
« Reply #1 on: October 08, 2008, 01:57:19 PM »
If I recall correctly, the sulfite is used to react with the peracid to form the acid and the sulfate. Peracids can be explosive if evaporated to dryness.

S

Sponsored Links