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Topic: Glycine  (Read 4127 times)

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Offline ethanham

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Glycine
« on: February 02, 2009, 10:22:39 PM »
I found that prolonged heating of glycine in the presence of quartz sand will produced glycyl-glycine, alaine, methylamine, aspartic acid, oxalic, succinic and fumaric. What about prolonged heating with only glycine at 170oC? What compound will be different?

TIA

Offline AWK

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Re: Glycine
« Reply #1 on: February 03, 2009, 12:54:44 AM »
Heating usally is not a good method for high yield synthesis. But heating glycin without catalyst vill give you a quite good yield of diketopiperazine first

http://en.wikipedia.org/wiki/Diketopiperazine
AWK

Offline Arkcon

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Re: Glycine
« Reply #2 on: February 03, 2009, 06:12:01 AM »
I found that prolonged heating of glycine in the presence of quartz sand will produced glycyl-glycine, alaine, methylamine, aspartic acid, oxalic, succinic and fumaric. What about prolonged heating with only glycine at 170oC? What compound will be different?

TIA

You got all that, from heating with sand.  Do your heating at 170 C, then just analyze again, and see what you get.
Hey, I'm not judging.  I just like to shoot straight.  I'm a man of science.

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