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Topic: Where to Buy a Safety Shield  (Read 8412 times)

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Offline Mitch

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Where to Buy a Safety Shield
« on: April 07, 2009, 07:09:19 PM »
Yes, I know I can google this. It didn't turn up any vendors I recognized. Suggestions? I'm going to be using sodium tert-butoxide and as we don't have any vertical sashes on the fume hood I want an extra layer of protection between me and the reaction.
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Offline kiwi

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Re: Where to Buy a Safety Shield
« Reply #1 on: April 07, 2009, 10:14:09 PM »
Personally I've only ever used standard PPE (gloves, googles, lab coat) with NaOtBu without problems. If you were really worried you could go with a full face shield, leaving you with no exposed skin. I presume you're worried about the corrosive nature of NaOtBu as opposed to what's going on in the reaction itself?

Offline gfunk

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Re: Where to Buy a Safety Shield
« Reply #2 on: April 07, 2009, 11:04:09 PM »
Have you tried Sigma-Aldrich?  Item #Z231363.  Or just search S-A for "safety shield" and get a whole whack of them :).  VWR and Fisher also carry them.
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Offline Mitch

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Re: Where to Buy a Safety Shield
« Reply #3 on: April 08, 2009, 01:52:32 PM »
kiwi: I've only used potassium t-BuLi before is sodium t-BuLi that different?
gfunk: Thanks, I'm checking them out now.
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Offline sjb

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Re: Where to Buy a Safety Shield
« Reply #4 on: April 08, 2009, 02:42:51 PM »
tBuLi or tBuOM (where M is a metal)?

Depends on the chemistry you're doing, but for most things there is probably little difference between the sodium and potassium salts.

Offline Mitch

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Re: Where to Buy a Safety Shield
« Reply #5 on: April 09, 2009, 03:12:22 PM »
sjb: I didn't think there was, thanks.
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