December 20, 2024, 09:30:07 PM
Forum Rules: Read This Before Posting


Topic: Separation and Purification experiment help  (Read 9335 times)

0 Members and 1 Guest are viewing this topic.

Offline cgc10

  • Very New Member
  • *
  • Posts: 1
  • Mole Snacks: +0/-0
Separation and Purification experiment help
« on: June 09, 2009, 07:18:10 PM »
I have to create a separation and purification scheme for a 3-component mixture composed of 2 neutral compounds and either an organic acid or base (ethyl-4-aminobenzoate/ benzil/ 1,4-dibromobenzene). The objective is to isolate 2 compounds in pure form.
I know extraction and crystallization are necessary, but what steps do I need to take in order to have the pure compounds? And in what order? Please please help, it's urgent!!

Offline spirochete

  • Chemist
  • Full Member
  • *
  • Posts: 547
  • Mole Snacks: +51/-9
  • Gender: Male
Re: Separation and Purification experiment help
« Reply #1 on: June 10, 2009, 02:40:24 PM »
You might get better results if you were more specific about what the neutral compounds are?

For the acid or base, look up acid/base extraction. You can exploit the drastically different solubilities of ionic and non ionic organic compounds to separate them.


Offline sjb

  • Global Moderator
  • Sr. Member
  • ***
  • Posts: 3653
  • Mole Snacks: +222/-42
  • Gender: Male
Re: Separation and Purification experiment help
« Reply #2 on: June 10, 2009, 03:20:24 PM »
You might get better results if you were more specific about what the neutral compounds are?


I thought they were mentioned -

... ethyl-4-aminobenzoate/ benzil/ 1,4-dibromobenzene...

?

All three are known compounds - is there anything in the Merck index or similar about the solubility or boliling point, for instance, of benzil / p-dibromobenzene?

Sponsored Links