December 28, 2024, 10:17:28 AM
Forum Rules: Read This Before Posting


Topic: Catalyst used in the Glovebox?  (Read 12646 times)

0 Members and 1 Guest are viewing this topic.

Offline Enantiomer

  • Regular Member
  • ***
  • Posts: 29
  • Mole Snacks: +2/-0
Catalyst used in the Glovebox?
« on: October 27, 2010, 09:40:03 PM »
Out of curiosity I've been looking for what catalyst it is that removes oxygen and water, I've heard that it is a 'Q5' catalyst but that doesn't ring a bell at all.

Anyone know?

Offline Doc Oc

  • Chemist
  • Full Member
  • *
  • Posts: 564
  • Mole Snacks: +48/-12
Re: Catalyst used in the Glovebox?
« Reply #1 on: October 28, 2010, 05:59:23 PM »
As far as I know it isn't a catalyst used to achieve this.  Oxygen is removed by repeatedly purging the box with nitrogen or argon.  I suppose dessicants can be added, maybe Drierite or something similar?  (It wasn't very humid at my school so we didn't worry as much about the moisture).

Offline MissPhosgene

  • Chemist
  • Full Member
  • *
  • Posts: 364
  • Mole Snacks: +23/-5
  • Gender: Female
Re: Catalyst used in the Glovebox?
« Reply #2 on: October 28, 2010, 09:05:24 PM »
There is a Q5 catalyst, produced by BASF and DOW, but I couldn't find out what it is. It might be a copper based catalyst.

Here is a link to a site where it is mentioned:

http://www.ilpi.com/inorganic/glassware/glovebox.html

Stereograms of the 32 crystallographic point groups: little bike wheels of cold, hard, pure rationality.

Offline Enantiomer

  • Regular Member
  • ***
  • Posts: 29
  • Mole Snacks: +2/-0
Re: Catalyst used in the Glovebox?
« Reply #3 on: October 29, 2010, 06:10:01 PM »
There is a Q5 catalyst, produced by BASF and DOW, but I couldn't find out what it is. It might be a copper based catalyst.

Here is a link to a site where it is mentioned:

http://www.ilpi.com/inorganic/glassware/glovebox.html
Yeah I saw this article too, I just figured that Q5 was a type or class of catalyst and wanted to know exactly the catalyst was

Offline macman104

  • Retired Staff
  • Sr. Member
  • *
  • Posts: 1644
  • Mole Snacks: +168/-26
  • Gender: Male
Re: Catalyst used in the Glovebox?
« Reply #4 on: November 02, 2010, 12:37:34 PM »
I believe Q5 is the actual catalyst that is used.  I found this paper, where they describe Q5 as 13% wt Cu(II)Oxide on Alumina.

http://dx.doi.org/10.1002/pola.20935

Offline 408

  • Chemist
  • Full Member
  • *
  • Posts: 796
  • Mole Snacks: +103/-30
Re: Catalyst used in the Glovebox?
« Reply #5 on: November 02, 2010, 01:25:19 PM »
I was always too lazy to do that in the gloveboxes I have used.  Instead I just left a lump of Na or K in the back in a beaker.

Offline wpenrose

  • Regular Member
  • ***
  • Posts: 35
  • Mole Snacks: +2/-0
  • Gender: Male
    • Custom Sensor Solutions, Inc.
Re: Catalyst used in the Glovebox?
« Reply #6 on: November 03, 2010, 09:37:39 PM »
Those hand warmers sold in hunting and hardware shops contain iron powder and a few other things to promote rapid oxidation. They're handy for creating a moderately oxygen-free environment.

DB
Custom Sensor Solutions, Inc.
Equipment and advice for users of chemical sensors.
http://www.customsensorsolutions.com

Sponsored Links