I boiled some sucrose solutions in test tubes for a high school lab last night. I had 5mL of roughly 1.5 molal sucrose solution in a test tube with a marble chip, but the thing still flash boiled and almost shot out of the tube. I count myself lucky.
First question: Even before the solution started boiling at all, it started making a rumbling noise as if it were boiling already. This was in test tubes with 5mL of 6 molal, 3 molal, and 1.5 molal sucrose. Is this noise a sign of super-heating? Are there any signs?
Second question: Were the test tubes a bad idea? Could the small exposed area have caused the solution to superheat?