It is very difficult to predict the mass of a solid from the volume in the way that you measured it. The solids are by nature irregular, and you have no idea how much of the volume was deadspace, empty air space between particles of solid. If you still have access to the teaspoon and the solids, the best choice would be to simply weigh out a teaspoonful of the solid, and just assume you were consistent enough to get relatively close to the same weight each time. The densities you will find in tables refer to the density of a solid mass of the material, not a crushed powder.
If you can't weigh the powder at this point, about all you can do is assume there was no airspace between the grains of the powder and look up the density of your solids. Then, since density is mass/volume, and you know the volume (roughly), you can calculate the mass (roughly).