Hey there! I need some help ASAP on a lab assignment on a back-titration of an unknown carbonate. I will provide the data obtained:
Mass of unknown carbonate samples:
Sample 1 2 3
Mass of vial + unknown 14.7803 g 14.6020 g 14.4273 g
Mass of vial 14.6020 g 14.4273 g 14.2418g
Mass of sample transferred 0.1783 g 0.1747 g 0.1855 g
Back-titrations with NaOH (50.00 mL standardized HCl added)
Sample 1 2 3
Final burette reading (mL) 24.61 44.71 43.72
Initial burette reading (mL) 4.91 24.61 28.04
Net volume of NaOH added (mL) 19.70 20.10 15.68
I calculated the concentration of NaOH to be 0.1212 mol/L and the mol of HCl in 50.00 mL to be 0.004908 mol. Also, I calculated the moles of NaOH needed to titrate the excess HCl in the flask as 0.002388 mol. I'm stuck with the following, please calculate (just for sample 1 only):
1. The moles of HCl remaining in flask 1 after the reaction with the unknown carbonate
2. The moles of HCl used up by the reaction with the unknown carbonate
3. The moles of carbonate ion that reacted.
4. The mass of carbonate ion that reacted.
5. The % Carbonate (by mass) in the unknown sample.