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Topic: Pd(PPh3)4  (Read 3869 times)

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Offline Senobim

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Pd(PPh3)4
« on: January 22, 2015, 04:37:03 PM »
Is it possible to recrystallize it? I found a bottle in the freezer and I am not sure about it's purity. (looks really orange) ;]
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Offline billnotgatez

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Re: Pd(PPh3)4
« Reply #1 on: January 22, 2015, 04:52:26 PM »
Just confirming you mean
http://en.wikipedia.org/wiki/Tetrakis%28triphenylphosphine%29palladium%280%29
Tetrakis(triphenylphosphine)palladium(0)
Pd[P(C6H5)3]4

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Offline Senobim

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Re: Pd(PPh3)4
« Reply #2 on: January 22, 2015, 04:56:55 PM »
indeed
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Offline sjb

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Re: Pd(PPh3)4
« Reply #3 on: January 22, 2015, 05:44:10 PM »
Definitely, from what I recall you can regenerate it from hydrazine (could be wrong, please check in Perrin and Ameregno or similar). Or why not try your reaction on a small scale first, it may still be OK
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