[Mpatas]

I tried this reaction today by using a mixture of sulfuric acid/Hydrogen peroxide but i was very confuse during the work up of the reaction. Some papers suggest to bacify the solution first and then extract it but i also found procedures that they just extract the reaction mixture. Is that possible? Can i get my product in the organic phase while it is acidic?

[kriggy]

Well try it. Ithink acidic conditions hels to keep the amine in aquaeous phase but it might depend on the specific molecule

[Dan]

Can i get my product in the organic phase while it is acidic?

It depends. Will the product be charge neutral under these conditions?