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Topic: Calculating Percent Yield for Cholesterol Lab  (Read 1520 times)

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Offline oliviagagnon

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Calculating Percent Yield for Cholesterol Lab
« on: November 06, 2019, 03:35:25 PM »
Hi everyone,

I am working on a lab report for the isolation of cholesterol lab. This experiment consisted of a series of four chemical reactions to convert pure cholesterol to 4-cholesten-3-one. First a bromination, then an oxidation, a debromination and finally as isomerization  using oxalic acid. I must calculate the percent yield for the intermediate 5-cholesten-3-one which was yielded after the debromination of dibromocholestanone using zinc powder. as well as the final product, 4-cholesten-3-one. I understand how to go about these calculations, however I can’t seem to find the balanced reactions for the debromination step or the isomerization step anywhere online. I need the stoichiometric coefficients of the two equations in order to calculate percent yield. Would anyone be able to help me with that?? Thank you in advance! 

Offline Babcock_Hall

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Re: Calculating Percent Yield for Cholesterol Lab
« Reply #1 on: November 06, 2019, 04:38:27 PM »
Think about what happens in an isomerization.

Offline oliviagagnon

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Re: Calculating Percent Yield for Cholesterol Lab
« Reply #2 on: November 06, 2019, 04:41:14 PM »
Think about what happens in an isomerization.
the same atoms are rearranged?

Offline Babcock_Hall

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Re: Calculating Percent Yield for Cholesterol Lab
« Reply #3 on: November 06, 2019, 05:16:27 PM »
Yes, and there is a simple inference that you can make from this information.

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