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Topic: Trying to make calcium acetate  (Read 1462 times)

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Offline some dude

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Trying to make calcium acetate
« on: April 17, 2020, 03:47:05 AM »
Hello,

I wanted to make calcium acetate from CaO and acetic acid. So I put 1 kg of burnt lime together with 1.5 l of acetic acid (98%) and some water. After it heavily reacted, I let it dry out and got a white powder. I thought it must be calcium acetate, but it is water insoluble. Calcium acetate would be soluble at about 300 g/l, this stuff does not dissolve at all. Does anyone know what that could be?

Offline chenbeier

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Re: Trying to make calcium acetate
« Reply #1 on: April 17, 2020, 07:57:37 AM »
Do you really got CaO and not gypsum?

Offline some dude

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Re: Trying to make calcium acetate
« Reply #2 on: April 17, 2020, 08:38:16 AM »
Label said burnt lime. Also, it started to boil when I was mixing it together. I thought it was because of a neutralisation reaction...

Offline OrganicDan96

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Re: Trying to make calcium acetate
« Reply #3 on: April 17, 2020, 01:14:17 PM »
probably excess calcium oxide, you are not using enough acetic acid

Offline Borek

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Re: Trying to make calcium acetate
« Reply #4 on: April 17, 2020, 02:41:27 PM »
probably excess calcium oxide, you are not using enough acetic acid

That would still react with water when trying to dissolve.

I agree there is not enough acetic acid.
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Offline OrganicDan96

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Re: Trying to make calcium acetate
« Reply #5 on: April 17, 2020, 03:03:07 PM »
probably excess calcium oxide, you are not using enough acetic acid

That would still react with water when trying to dissolve.

I agree there is not enough acetic acid.

calcium hydroxide has a solubility of 1.73 g/l at 20°C

Offline some dude

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Re: Trying to make calcium acetate
« Reply #6 on: April 18, 2020, 05:23:33 AM »
Right, must be CaO/CaOH then, thanks.

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