November 22, 2024, 07:59:10 AM
Forum Rules: Read This Before Posting


« previous next »
Pages: [1]   Go Down

Topic: Phenol from Anisol with HBr 48%  (Read 1621 times)

0 Members and 2 Guests are viewing this topic.

Offline Qxir09

  • Very New Member
  • *
  • Posts: 1
  • Mole Snacks: +0/-0
Phenol from Anisol with HBr 48%
« on: September 04, 2023, 01:25:00 PM »
Hello,
i want to make Phenol from Anisol with HBr 48% (i don't have HI, i have AlCl3 but no Chorobenzene).
As far as i know, it doesn't work at room temp.

How long should i reflux and at which temp?
Logged

Offline Babcock_Hall

  • Chemist
  • Sr. Member
  • *
  • Posts: 5704
  • Mole Snacks: +330/-24
Re: Phenol from Anisol with HBr 48%
« Reply #1 on: September 05, 2023, 01:28:53 PM »
Do you have access to SciFinder or an equivalent tool?  This would be the best way to obtain conditions.  Why do you want to make something that you can buy?
Logged

Offline rolnor

  • Chemist
  • Sr. Member
  • *
  • Posts: 2299
  • Mole Snacks: +154/-10
Re: Phenol from Anisol with HBr 48%
« Reply #2 on: September 15, 2023, 10:23:54 PM »
It usually takes 1hour.
Logged

Offline rolnor

  • Chemist
  • Sr. Member
  • *
  • Posts: 2299
  • Mole Snacks: +154/-10
Re: Phenol from Anisol with HBr 48%
« Reply #3 on: September 17, 2023, 04:08:46 AM »
And reflux gives you the right temp.
Logged
Pages: [1]   Go Up
« previous next »
Sponsored Links