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Topic: catalyst for producing benzotrichloride  (Read 3093 times)

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Offline previnz

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catalyst for producing benzotrichloride
« on: August 22, 2007, 08:47:03 AM »
dear freinds, ???
i am in production of benzotrichloride. At present by the method of chlorination of toluene in presence of ultraviolet bulbs i am able to get benzotrichloride in 30 hrs reaction time, which is very slow  :-[. I would like you to suggest me the name of a few catalysts which could speed up my reation time considerably  :).
thanks

Offline chengyang79

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Re: catalyst for producing benzotrichloride
« Reply #1 on: September 03, 2007, 01:07:04 PM »
Try to add catalytic amount of PCl3 and 2,2'-Azobisisobutyronitrile(AIBN) into the  reaction system will be better.

And also the UV light maybe absorbed by normal glass reactor .It is better to use a flask which made by quartz glass.


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