My lab instructor asked me a simple question about what temperature I'd expect during the steam distillation I was doing. I was finishing up my Sandmeyer reaction of CuCl with my o-toluidine and the NO
2 and basically doing steam distillation on that before doing the separation process work-up (by adding acid then base, removing the color, etc).
Anyways, I told my instructor that it would be around 100 degrees since it had mostly water in it and that the water will boil before the product does because it has a higher boiling point than water.
Then, the instructor got really shocked/mad (funny and scary
) and demanded a proper answer the next time I see her. She said there's something special about steam distillation compared to the regular simple distillation but she didn't tell me.
(sorry for edit, accidently pressed enter and it saved)
So I'm obviously not getting it about steam distillation
If it's boiling at 100 degrees due to water, and the product has a higher boiling point than that, then the water will just simply boil with my product into my collection flask. So, I don't see how this is special since it looks like a purification process to me. Any ideas what she might've meant?