December 22, 2024, 12:26:12 PM
Forum Rules: Read This Before Posting


Topic: how do I purify a thiosemicarbazone ligand?  (Read 3549 times)

0 Members and 1 Guest are viewing this topic.

Offline smurf88

  • New Member
  • **
  • Posts: 4
  • Mole Snacks: +0/-0
how do I purify a thiosemicarbazone ligand?
« on: January 20, 2010, 02:07:47 AM »
I am trying to produce a semicarbazone ligand.
The melting point should be around 145 to 146 Celcius.
But the ligand that I obtained is around 196C.
I tried to purify it by washing with methanol.
Or is there any better method to purify my ligand?

Offline verpa

  • New Member
  • **
  • Posts: 7
  • Mole Snacks: +1/-0
  • Gender: Male
Re: how do I purify a thiosemicarbazone ligand?
« Reply #1 on: April 02, 2010, 11:32:19 AM »
This one is a bit old ( was just checking out your other posts ) but if you have this sort of question in the future, you might also cross post to:
http://lab.chempedia.com

fwiw.

Sponsored Links