January 15, 2025, 09:50:26 PM
Forum Rules: Read This Before Posting


Topic: Recrystalization reactions and mechanisms  (Read 5446 times)

0 Members and 1 Guest are viewing this topic.

tiger17

  • Guest
Recrystalization reactions and mechanisms
« on: October 05, 2005, 11:09:13 AM »
We had to recrystalize benzoic acid, I'm having a hard time figuring out what the reaction is because we only used benzene, water, and charcoal.  This was our procedure:

1. Add 1 g impure benzoic acid + 15 mL water
2. Heat with condenser
3. Add little more water
4. Cool
5. Add a little carbon
6. Reheat
7. Hot filtration
8. Ice water bath
9. Vaccum filter

Offline sundberg

  • Regular Member
  • ***
  • Posts: 33
  • Mole Snacks: +5/-0
  • I'm a mole!
Re:Recrystalization reactions and mechanisms
« Reply #1 on: October 05, 2005, 01:58:29 PM »
The theory behind recrystallisation doesn't involve any mechanisms, it's just based on solving the compound being purified in a suitable solvent and then allowing it to cool slowly to allow reformation of crystals. This way impurities doesn't get trapped, which is the case when crystallization is instantaneous/fast.

Active charcoal also traps impurities, and is often used to remove miscolorations of compounds etc.

tiger17

  • Guest
Re:Recrystalization reactions and mechanisms
« Reply #2 on: October 05, 2005, 05:30:34 PM »
I know, that's why I was confused.  So is there also no reaction?

Offline sundberg

  • Regular Member
  • ***
  • Posts: 33
  • Mole Snacks: +5/-0
  • I'm a mole!
Re:Recrystalization reactions and mechanisms
« Reply #3 on: October 05, 2005, 06:07:45 PM »
Not except solving of the crystals. :)


Sponsored Links