[benjamin5476]

I want to do an organic reaction of high pressure,But I can not find the requirements of equipment,I want to achieve pressure is 60kgf/cm2,What kind of equipment is more appropriate??

[discodermolide]

What scale will the reaction be?

[fledarmus]

If you got to the Sigma-Aldrich website and search for "pressure reactor", you will find several varieties rated for different pressures. I have found the following type to be most convenient for small scale lab work, but they use over-heated solvents for pressure and have no provision for adding additional gas for pressure.

http://www.sigmaaldrich.com/catalog/product/aldrich/z181099?lang=en&region=US&cm_sp=Customer_Favorites-_-Detail_Page-_-Image-Z181099

I have also used something similar to this when I needed to use high pressure gas in the reaction. In my case it was ammonia.

http://www.berghof.com/Products/en/Products/Laboratory+Instruments/High+Pressure+Reactors-p-3011.html

[benjamin5476]

What scale will the reaction be?

The reaction scale is 2 L,Do you have any suggestions?

[discodermolide]

Look in Google for the equipment. Pressure reactors: for example: http://syrris.com/batch-products/atlas-pressure-reactors?_kk=pressure%2520reactors&_kt=8c2e207e-0ee7-4809-a2c1-609abdff90e0&gclid=CMHygICl0bICFcRV3godalgAgA

[fledarmus]

Wow, 2L pressure reactor - that almost takes it out of laboratory scale. You might want to check with whoever your facilities manager is to be sure you can run that large a reaction under that much pressure inside your lab. Many labs and especially lab hoods aren't rated for containing pressure if there is a rupture.

It also takes you well beyond the glass pressure vessels. You will probably be searching for either a stainless steel pressure reactor or a glass lined pressure reactor. A quick google search turns up lots of suppliers for both.

Unfortunately, my last experience with a pressure reactor that size was nearly 30 years ago, and the reactor was an obsolete piece of equipment then. I don't think my input will be very helpful.

[discodermolide]

Have a look here, they may have something you can use.
http://syrris.com/batch-products/atlas-pressure-reactors?_kk=pressure%2520reactors&_kt=8c2e207e-0ee7-4809-a2c1-609abdff90e0&gclid=CMHygICl0bICFcRV3godalgAgA

[orgopete]

Wow, 2L pressure reactor - that almost takes it out of laboratory scale. You might want to check with whoever your facilities manager is to be sure you can run that large a reaction under that much pressure inside your lab. Many labs and especially lab hoods aren't rated for containing pressure if there is a rupture.

I agree with this comment. Although I have not done many high pressure reactions and of them were on a large scale, safety really needs to be addressed. I have seen the results of high pressure ruptures. I always have a lot of anxiety with these reactions, especially at the start and end when you have to expose yourself to what may be a high pressure vessel. Why do you think the vessel may also be referred to as a bomb? If so, then a 2L vessel might be referred to as a big bomb.

[curiouscat]

I've used Parr reactors; very convenient.

Here's a 2 L, 200 bar model:

http://www.parrinst.com/products/stirred-reactors/series-4520-1-2l-bench-top-reactors/

[curiouscat]

Look in Google for the equipment. Pressure reactors: for example: http://syrris.com/batch-products/atlas-pressure-reactors?_kk=pressure%2520reactors&_kt=8c2e207e-0ee7-4809-a2c1-609abdff90e0&gclid=CMHygICl0bICFcRV3godalgAgA

Why are they called "Atlas Sodium Pressure" and "Atlas Potassium Pressure". They use the molten  metals as a heating medium?

I was intrigued by the reference to Alkali Metals in their names. 

[discodermolide]

No idea, certainly not what you suggest.
Why do you have Escort as a name for a car or Astra or any other name. Why is your name curiouscat?

[curiouscat]

Why do you have Escort as a name for a car or Astra or any other name. Why is your name curiouscat?

That itself is one satisfactory explanation. I read more into it than there was.