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Convenient preparation of allyl bromide
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Topic: Convenient preparation of allyl bromide (Read 4454 times)
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AFFA
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Convenient preparation of allyl bromide
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on:
December 27, 2005, 02:12:21 PM »
Hi all,
I encounter trouble in preparing allyl bromide (Deuterium-labelled). My starting material is d-labelled alcohol. Since b.p. of allyl bromide and diethyl ether is 70 oC and 35 oC respectively, I worried about a significant loss upon fractional distillation. Is this a good approach to make my allyl bromide? Any other suggestions? I hope some of you could give me some suggestions in my situation.
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ksr985
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Re:Convenient preparation of allyl bromide
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December 27, 2005, 02:14:43 PM »
i am curious. assuming that youre distlling your product mixture reasonably slowly, isnt 35 degrees a good enough temperature difference at such low temperatures?
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Convenient preparation of allyl bromide