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Silver nitrate in dessicator bag
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Topic: Silver nitrate in dessicator bag (Read 3852 times)
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Tittywahah
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Silver nitrate in dessicator bag
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on:
December 07, 2012, 08:13:46 AM »
In an attempt to purify synthesized Silver nitrate I have re-dissolved it in De-ionized water. Though in order to speed up the evaporation I was wondering whether Sodium Hydroxide in a dessicator bag with the silver nitrate would have any adverse effects? I usually use the NaOH for absorbing acidic gases and water from various things but not sure about such a precious product where I can not afford to lose anything. Thankyou.
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curiouscat
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Re: Silver nitrate in dessicator bag
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Reply #1 on:
December 07, 2012, 08:56:08 AM »
Why not mild heat?
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Tittywahah
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Re: Silver nitrate in dessicator bag
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Reply #2 on:
December 07, 2012, 09:32:42 AM »
Quote from: curiouscat on December 07, 2012, 08:56:08 AM
Why not mild heat?
Yes I know but I guess I am reluctant to involve heat when it coms to silver nitrate because of the ease with which it decomposes and since I could not find the temperature at which it decomposes I relied on some vague distant memory notion that it was just 60/70c.
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curiouscat
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Re: Silver nitrate in dessicator bag
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Reply #3 on:
December 07, 2012, 09:42:53 AM »
Do you have a wet solid sample that you want to dry? Or a liquid solution you want to evaporate H2O out of?
Could you apply a vacuum?
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Tittywahah
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Re: Silver nitrate in dessicator bag
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Reply #4 on:
December 07, 2012, 10:02:40 AM »
Wet solid sample would evaporate easily, I would never heat that. No, I have about 75mLs water to evaporate. I decided to go ahead anyway, it's on a hotplate. No access to a vacuum I'm afraid. I know they are handy for some things I do.
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curiouscat
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Re: Silver nitrate in dessicator bag
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Reply #5 on:
December 07, 2012, 11:31:01 AM »
Be careful. I think AgNO3 has been known to detonate in certain conditions. EtOH being one.
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Tittywahah
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Re: Silver nitrate in dessicator bag
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Reply #6 on:
December 07, 2012, 12:33:38 PM »
Yes I know, but thought that was only in direct contact. anyway, decided to use the slow boat method - I'll leave it to evaporate naturally.
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Silver nitrate in dessicator bag