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Topic: How to synthesize peroxide bond????  (Read 1400 times)

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Offline linh_ngt

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How to synthesize peroxide bond????
« on: February 25, 2014, 12:06:41 PM »
Hello all,
I would like to synthesize peroxide bonds from the nosylate compounds (-OSO2R into -OOH or OOtBu)? Does any of you have any recommendation for this kind of reactions?
Actually, I already tried with H2O2 in Na2CO3 and tBuOOH in K2CO3, but nothing works at all.
Now I am trying with NaH and tBuOOH in dry THF.
I am really appreciated with your *delete me*!!
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Offline TheUnassuming

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Re: How to synthesize peroxide bond????
« Reply #1 on: February 25, 2014, 02:13:42 PM »
Not sure I'm understanding you correctly. 
Can you give more info on the substrates you are wanting to form into peroxides?
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When in doubt, avoid the Stille coupling.
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