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Topic: triethyl amine purfication after column  (Read 1367 times)

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Offline saubanzaheer

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triethyl amine purfication after column
« on: April 15, 2014, 11:41:25 AM »
I purified my compound possess one free NH2 group on column by using triethyl amine. Now I have problem because the TEA strong signal in proton NMR is appeared along with my compound. Can any one help me how to remove this from my compound.
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Offline Archer

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Re: triethyl amine purfication after column
« Reply #1 on: April 15, 2014, 03:22:57 PM »
What is your molecule with one amine? You could use high vacuum if it's not too volatile.
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