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any valuable reference for purification of organic compounds
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Topic: any valuable reference for purification of organic compounds (Read 1661 times)
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ABA2015
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any valuable reference for purification of organic compounds
«
on:
May 06, 2014, 03:00:33 AM »
hi all
I'm interested to find a valuable book in purification of compounds especially in crystallization of organic compounds, can you introduce me any?
thanks
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Dan
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Organic Chemist
Re: any valuable reference for purification of organic compounds
«
Reply #1 on:
May 06, 2014, 05:05:27 AM »
How advanced and/or in depth are you looking for?
Zubrick's lab survival manual
is a great book for inexperienced chemists,
Vogel's is a handy tome
.
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TheUnassuming
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Re: any valuable reference for purification of organic compounds
«
Reply #2 on:
May 06, 2014, 12:22:37 PM »
I second both of those references for good general guides to various wet lab procedures. Zubricks is a bit smaller but a good starting point most of the common things you will need to do. Vogals is bigger and more detailed, but in certain parts can be a bit out-dated as techniques have progressed as new equipment has become commonly available.
You can always start with the original flash chromotography paper:
http://pubs.acs.org/doi/abs/10.1021/jo00408a041
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When in doubt, avoid the Stille coupling.
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any valuable reference for purification of organic compounds