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3-methyl-butyrolactone
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Topic: 3-methyl-butyrolactone (Read 6350 times)
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sohushi
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3-methyl-butyrolactone
«
on:
March 22, 2006, 02:40:42 AM »
how to make the compound
wait for your repay
«
Last Edit: March 22, 2006, 10:53:58 PM by sohushi
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AWK
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Re:3-methyl-butyrolactone
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Reply #1 on:
March 22, 2006, 03:35:36 AM »
Start from sketch of its structure
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Last Edit: March 22, 2006, 03:38:49 AM by AWK
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Albert
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Re:3-methyl-butyrolactone
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Reply #2 on:
March 22, 2006, 01:21:29 PM »
From which compound(s) do you have to start?
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HP
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Re:3-methyl-butyrolactone
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Reply #3 on:
March 22, 2006, 02:10:04 PM »
Butyrolactone can be easily prepared from tetrahydrofuran (THF) when oxidize with Ca-hypochlorite ( Ca(OCl)2) or HNO3 as oxidizing agents.
Well may be if you start from methyl-THF...For the synthesis this you may start from furfural ( produced commercially by the acid hydrolysis of pentosan polysaccharides from non-food residues of food crops and wood wastes) then convert aldehyde CHO group to CH3(now i dont have exact idea this reaction) and of course hydrogenation of the double bonds
Hope this compound isn't drug precursor for bad aims!
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sohushi
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Re:3-methyl-butyrolactone
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Reply #4 on:
March 22, 2006, 09:47:21 PM »
I want to start from 2-methyl-1,3-propanediol .
how can you prepared from tetrahydrofuran (THF) when oxidize with Ca-hypochlorite ( Ca(OCl)2) or HNO3 as oxidizing agents.
please speak in detail .
do you have some reference literature .
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AWK
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Re:3-methyl-butyrolactone
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Reply #5 on:
March 23, 2006, 02:15:48 AM »
(17) (a) Schulz, S. Liebigs Ann. Chem. 1992, 829. (b) Kayser, M. M.;
Morand, P. Can. J. Chem. 1980, 58, 2484.
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3-methyl-butyrolactone