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Topic: Trying to crystallize a salt in solution  (Read 2247 times)

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Offline blueberry58

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Trying to crystallize a salt in solution
« on: February 06, 2015, 12:59:25 PM »
I have prepared some magnesium thiosulfate using magnesium sulfite and elemental sulfur 1:1 mole ratio with strong agitation for 4 hours. This product is unstable on heating. If I heat this clear solution to achieve its crystallization, sulfur returns to form.
I decided use just low heat ( 60 degrees) and it become a kind of jam that does not crystallize. On heating it returns to liquid state. What should I do in this case?

Thank you.

Offline Borek

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Re: Trying to crystallize a salt in solution
« Reply #1 on: February 06, 2015, 01:51:05 PM »
Vacuum?

Or just wait till it dries out in the room temperature?
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Offline blueberry58

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Re: Trying to crystallize a salt in solution
« Reply #2 on: February 07, 2015, 11:41:37 AM »
Yes. I just left it to dry at the darkness.
Thank you Borek.

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