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Seperating amine salt from sulfonyl amide
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Topic: Seperating amine salt from sulfonyl amide (Read 1608 times)
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lux94
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Seperating amine salt from sulfonyl amide
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on:
November 06, 2015, 02:49:10 PM »
Hello fellow chemists,
today by a mistake i mixed wrong flasks together, and contaminated my pure product.Now i have mixture of amine trifluoroacetate salt (like 80%) and sulfonyl amide.I guess there is no point of performing chromatografy, because amine salt is way too polar.I was thinking perhaps there is a way, that i could extract amine salt from organic phase with water? What could be right conditions for the salt to dissolve in water? Im adding an image of structure of molecues.
http://www.bildites.lv/viewer.php?file=5pff3lkl83crr2twtrud.jpg
Thank you for your replies beforehand.
-L
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kriggy
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Re: Seperating amine salt from sulfonyl amide
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November 06, 2015, 03:22:53 PM »
If your salt is soluble in water while the other compound is not then its easy. I think chromatography might work too - you firstly elute your starting material and then your salt using methanol with some base
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Seperating amine salt from sulfonyl amide